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High Production Rate Synthesis of CdS Nanoparticles Using a Reverse Oscillatory Flow Method

[+] Author Affiliations
Daniel A. Peterson, C. Padmavathi, Brian K. Paul

Oregon State University, Corvallis, OR

Paper No. MSEC2014-3957, pp. V001T03A004; 10 pages
doi:10.1115/MSEC2014-3957
From:
  • ASME 2014 International Manufacturing Science and Engineering Conference collocated with the JSME 2014 International Conference on Materials and Processing and the 42nd North American Manufacturing Research Conference
  • Volume 1: Materials; Micro and Nano Technologies; Properties, Applications and Systems; Sustainable Manufacturing
  • Detroit, Michigan, USA, June 9–13, 2014
  • Conference Sponsors: Manufacturing Engineering Division
  • ISBN: 978-0-7918-4580-6
  • Copyright © 2014 by ASME

abstract

A reverse oscillatory flow (ROF) mixing system is discussed having a reaction channel 460 μm high by 152 mm wide for high flow rate processing of nanoparticle chemistries. The ROF system is demonstrated to produce CdS nanoparticles at a production rate of 115.7 g/hour with a coefficient of variation for particle size down to 19%. These production rates are substantially higher than those achieved using other microchannel mixers while maintaining comparable size distributions. Advantages of the ROF approach include the use of larger microchannels which make the reactor easier to fabricate and less vulnerable to clogging.

Copyright © 2014 by ASME

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