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Solid-State Foaming of Polycaprolactone (PCL)

[+] Author Affiliations
Hai Wang, Wei Li, Vipin Kumar

University of Washington, Seattle, WA

Paper No. IMECE2007-42666, pp. 61-66; 6 pages
doi:10.1115/IMECE2007-42666
From:
  • ASME 2007 International Mechanical Engineering Congress and Exposition
  • Volume 3: Design and Manufacturing
  • Seattle, Washington, USA, November 11–15, 2007
  • Conference Sponsors: ASME
  • ISBN: 0-7918-4297-5 | eISBN: 0-7918-3812-9
  • Copyright © 2007 by ASME

abstract

Polycaprolacton (PCL) is a synthetic biodegradable polymer that is widely used in tissue engineering related studies. It is a semi-crystalline polymer, and has a glass transition temperature (Tg ) of −60°C and a melting temperature of 60°C. In this paper, we report on the progress in creating porous PCL foams using the solid-state foaming process. The objective of this study is to examine the foam-ability of PCL using room temperature saturation. PCL specimens were made using compression molding. A “quenching” process was introduced to manipulate the crystallinity of PCL samples. CO2 was used for gas saturation. The effects of saturation pressure and foaming temperature were studied. The created microstructures were characterized using scanning electron microscopy (SEM). The preliminary results have shown that microstructures with pores on the scale of hundreds of nanometers were generated.

Copyright © 2007 by ASME

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